Artikel Jurnal :: Kembali

Artikel Jurnal :: Kembali

Synthesis of lithium titanate (li4Ti5O12) through hydrothermal process by using lithium hydroxide (lioh) and titanium dioxide (Tio2) xerogel

Anne Zulfia Syahrial, Akhmad Herman Yuwono, Evvy Kartini, Mario Marfelly, Wahid Muhamad Furkon Rahmatulloh (Faculty of Engineering, Universitas Indonesia, 2015)

 Abstrak

Lithium Titanate (Li4Ti5O12) or (LTO) has a potential as an anode material for a high performance lithium ion battery. In this work, LTO was synthesized by a hydrothermal method using Titanium Dioxide (TiO2) xerogel prepared by a sol-gel method and Lithium Hydroxide (LiOH). The sol-gel process was used to synthesize TiO2 xerogel from a titanium tetra-n-butoxide/Ti(OC4H9)4 precursor. An anatase polymorph was obtained by calcining the TiO2 xerogel at a low temperature, i.e.: 300oC and then the hydrothermal reaction was undertaken with 5M LiOH aqueous solution in a hydrothermal process at 135oC for 15 hours to form Li4Ti5O12. The sintering process was conducted at a temperature range varying from 550oC, 650oC, and 750oC, respectively to determine the optimum characteristics of Li4Ti5O12. The characterization was based on Scanning Thermal Analysis (STA), X-ray Powder Diffraction (XRD), Field Emission Scanning Electron Microscopy (FESEM), Fourier Transform Infrared spectroscopy (FTIR), and Brunauer-Emmett-Teller (BET) testing results. The highest intensity of XRD peaks and FTIR spectra of the LTO were found at the highest sintering temperature (750oC). As a trade-off, however, the obtained LTO/Li4Ti5O12 possesses the smallest BET surface area (< 0.001 m2/g) with the highest crystallite size (56.45 nm).

 Metadata

Jenis Koleksi : Artikel Jurnal
No. Panggil : UI-IJTECH 6:4 (2015)
Entri utama-Nama orang :
Subjek :
Penerbitan : Depok: Faculty of Engineering, Universitas Indonesia, 2015
Sumber Pengatalogan : LibUI eng rda
ISSN : 20869614
Majalah/Jurnal : International Journal of Technology
Volume : Vol. 6, No. 4, October 2015: Hal. 555-564
Tipe Konten : text
Tipe Media : unmediated
Tipe Carrier : volume
Akses Elektronik : https://doi.org/10.14716/ijtech.v6i4.1965
Institusi Pemilik : Universitas Indonesia
Lokasi : Perpustakaan UI, Lantai 4 R. Koleksi Jurnal
  • Ketersediaan
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No. Panggil No. Barkod Ketersediaan
UI-IJTECH 6:4 (2015) 08-23-54711551 TERSEDIA
Ulasan:
Tidak ada ulasan pada koleksi ini: 9999920521624
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