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A new precipitation-hardened austenitic stainless steel investigated by electron microscopy

Parikin Parikin, Arbi Dimiyati, Dr. Abu Khalid Rivai, Riza Iskandar (Faculty of Engineering, Universitas Indonesia, 2018)

 Abstract

The 56Fe16.6Cr25Ni0.9Si0.5Mn austenitic superalloy has been produced in an induction furnace; it was made from granular ferro-scrap, ferrochrome, ferrosilicon, and ferromanganese materials. Originally, this alloy had been proposed for use in high mechanical loads and high temperature conditions (such as in nuclear and fossil fuel power plant facilities). Tensile strength tests showed that the alloy has an average yield strength of about 430.56 MPa, which is higher than Incoloy A-286 (a commercially available alloy). A combination of microscopy techniques by means of an optical microscope, X-ray diffraction [XRD], scanning electron microscopy [SEM], and transmission electron microscopy [TEM] techniques were applied in order to get detailed information about the fine structure of the alloy. XRD confirmed that the alloy matrix exhibits an FCC crystal structure with a lattice parameter of about 3.60 Å and grain sizes ranging from 50 to 100 µm. The results of the TEM analysis revealed the new type of precipitations that formed at the grain boundaries. These needle-like precipitations, probably Fe/Cr-rich precipitations of the (Fe,Cr)xCy type, acted as the source of intergranular corrosion (IGC). Small coherent plate-like and much smaller granular precipitations were found distributed homogenously along grain boundaries and inside the grains. Combining the tensile strength test and microstructure analysis suggested that these precipitations play significant roles in the hardness of the investigated sample.

 Metadata

Collection Type : Artikel Jurnal
Call Number : UI-IJTECH 9:1 (2018)
Main entry-Personal name :
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Publishing : Depok: Faculty of Engineering, Universitas Indonesia, 2018
Cataloguing Source : LibUI eng rda
ISSN : 20869614
Magazine/Journal : International Journal of Technology
Volume : Vol. 9, No. 1, January 2018: Hal. 89-98
Content Type : text
Media Type : unmediated
Carrier Type : volume
Electronic Access : https://doi.org/10.14716/ijtech.v9i1.888
Holding Company : Universitas Indonesia
Location : Perpustakaan UI, Lantai 4 R. Koleksi Jurnal
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Call Number Barcode Number Availability
UI-IJTECH 9:1 (2018) 08-23-58715887 TERSEDIA
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No review available for this collection: 9999920522073
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