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"[ABSTRAKPenelitian ini dilakukan untuk mengetahui pengaruh sonikasi dengan media air terhadap serbuk timbal sebagai material aktif elektroda positif (PAM) dan hubunganya terhadap kapasitas baterai lead acid. Serbuk timbal yang dipakai merupakan standar pabrik yang di produksi dengan metode ball mill (Shimadzu). Serbuk timbal hasil sonikasi kemudian dianalisa dengan Partikel Size Analizer (PSA), X-ray diffraction ( XRD), GSAS, SEM/EDS dan Gravimetric Free Lead Test. Aglomerasi serbuk timbal terjadi pada awal proses sonikasi. Telah didapat serbuk timbal dengan ukuran nano (92 nm) pada sonikasi 600 menit. Serbuk timbal hasil sonikasi digunakan sebagai elektroda positif yang dipasangkan dengan elektroda negarif dari standar pabrik. Kapasitas mula yang dihasilkan ternyata lebih kecil dari kapasitas standar pabrik hal ini karena hilangnya komponen free lead pada serbuk timbal hasil sonikasi. Semakin kecil free lead yang terkandung dalam serbuk timbal hasil sonikasi dengan media air, PAM secara mekanik tidak stabil, proses formasi sulit dan kapasitas baterai yang dihasilkan semakin kecil. Ditemukan pula bahwa semakin besar ukuran partikel serbuk timbal sebagai bahan material aktif positif maka umur pakai baterai semakin baik.

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ABSTRACTOur goal in this research was to determine the effect of sonication leady oxide with distilled water as positive active material (PAM) and relation to the lead acid batteries capacity. Industrial product leady oxide (ball mill method) was used as raw material in this research. The prepared leady oxide was characterized and analyzed by particle size analyzer (PSA), X-ray diffraction (XRD), GSAS, SEM/EDS and Gravimetric Free Lead Test. Agglomeration occurs at the beginning of sonication. Been obtained the nanostructure leady oxide with particle size 92 nm at 600 minutes sonication. It?s sonication results are used as positive electrode which coupled with industrial negatives plates. The resulting initial capacity is smaller than Industrial product because loss of free lead components on leady oxide sonication results. The lack of free lead components in leady oxide as a result of water solvent sonication, cause PAM is mechanically unstable and difficult to form, and hence the plates have lower capacity. It was also obtained that larger particle size of leady-oxide , the life cycle of the battery is getting better;Our goal in this research was to determine the effect of sonication leady oxide with distilled water as positive active material (PAM) and relation to the lead acid batteries capacity. Industrial product leady oxide (ball mill method) was used as raw material in this research. The prepared leady oxide was characterized and analyzed by particle size analyzer (PSA), X-ray diffraction (XRD), GSAS, SEM/EDS and Gravimetric Free Lead Test. Agglomeration occurs at the beginning of sonication. Been obtained the nanostructure leady oxide with particle size 92 nm at 600 minutes sonication. It?s sonication results are used as positive electrode which coupled with industrial negatives plates. The resulting initial capacity is smaller than Industrial product because loss of free lead components on leady oxide sonication results. The lack of free lead components in leady oxide as a result of water solvent sonication, cause PAM is mechanically unstable and difficult to form, and hence the plates have lower capacity. It was also obtained that larger particle size of leady-oxide , the life cycle of the battery is getting better;Our goal in this research was to determine the effect of sonication leady oxide with distilled water as positive active material (PAM) and relation to the lead acid batteries capacity. Industrial product leady oxide (ball mill method) was used as raw material in this research. The prepared leady oxide was characterized and analyzed by particle size analyzer (PSA), X-ray diffraction (XRD), GSAS, SEM/EDS and Gravimetric Free Lead Test. Agglomeration occurs at the beginning of sonication. Been obtained the nanostructure leady oxide with particle size 92 nm at 600 minutes sonication. It’s sonication results are used as positive electrode which coupled with industrial negatives plates. The resulting initial capacity is smaller than Industrial product because loss of free lead components on leady oxide sonication results. The lack of free lead components in leady oxide as a result of water solvent sonication, cause PAM is mechanically unstable and difficult to form, and hence the plates have lower capacity. It was also obtained that larger particle size of leady-oxide , the life cycle of the battery is getting better;Our goal in this research was to determine the effect of sonication leady oxide with distilled water as positive active material (PAM) and relation to the lead acid batteries capacity. Industrial product leady oxide (ball mill method) was used as raw material in this research. The prepared leady oxide was characterized and analyzed by particle size analyzer (PSA), X-ray diffraction (XRD), GSAS, SEM/EDS and Gravimetric Free Lead Test. Agglomeration occurs at the beginning of sonication. Been obtained the nanostructure leady oxide with particle size 92 nm at 600 minutes sonication. It’s sonication results are used as positive electrode which coupled with industrial negatives plates. The resulting initial capacity is smaller than Industrial product because loss of free lead components on leady oxide sonication results. The lack of free lead components in leady oxide as a result of water solvent sonication, cause PAM is mechanically unstable and difficult to form, and hence the plates have lower capacity. It was also obtained that larger particle size of leady-oxide , the life cycle of the battery is getting better, Our goal in this research was to determine the effect of sonication leady oxide with distilled water as positive active material (PAM) and relation to the lead acid batteries capacity. Industrial product leady oxide (ball mill method) was used as raw material in this research. The prepared leady oxide was characterized and analyzed by particle size analyzer (PSA), X-ray diffraction (XRD), GSAS, SEM/EDS and Gravimetric Free Lead Test. Agglomeration occurs at the beginning of sonication. Been obtained the nanostructure leady oxide with particle size 92 nm at 600 minutes sonication. It’s sonication results are used as positive electrode which coupled with industrial negatives plates. The resulting initial capacity is smaller than Industrial product because loss of free lead components on leady oxide sonication results. The lack of free lead components in leady oxide as a result of water solvent sonication, cause PAM is mechanically unstable and difficult to form, and hence the plates have lower capacity. It was also obtained that larger particle size of leady-oxide , the life cycle of the battery is getting better]"

"Liposom sebagai sistem penghantaran obat yang baik pelu menjaga kestabilan ukurannya. Metode pengecilan ukuran liposom yang umum digunakan adalah ekstrusi dan sonikasi. Pada penelitian ini bertujuan membandingkan pengecilan ukuran dengan metode ekstrusi bertingkat dengan melewatkan suspensi liposom melalui membran polikarbonat 0,45 μm sebanyak satu siklus, dilanjutkan dengan melewatkan suspensi liposom melalui membran polikarbonat 0,22 μm sebanyak 3,6, dan 9 siklus dan metode sonikasi selama 10, 20 dan 30 menit. Setelah dievaluasi distribusi ukuran liposom dan efisiensi penjerapan liposom, diperoleh liposom hasil ekstrusi 6 siklus dan sonikasi 10 menit mempunyai hasil yang terbaik yang kemudian digunakan dalam formulasi gel. Setelah diformulasi ke dalam gel, gel yang mengandung liposom hasil ekstrusi 6 siklus mengalami peningkatan ukuran sebesar 7,71 kali dan gel yang mengandung liposom hasil sonikasi selama 10 menit mengalami peningkatan ukuran sebesar 12,18 kali. Hal ini memperlihatkan bahwa gel yang mengandung liposom hasil ekstrusi menunjukkan hasil pengecilan yang lebih baik dibandingkan gel yang mengandung liposom hasil sonikasi.

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Liposome as a good drug delivery system need to maintain a stable size. Liposome size reduction method that mostly use is extruction and sonication. The aimed of this research is to compare size reduction method using two step of extruction by extruded liposome suspension through 0,45 μm polycarbonate membrane 1 cycle and then extruded it through 0,22 μm polycarbonate membrane 3, 6, and 9 cycles and sonication method for 10, 20, and 30 minutes.

Result showed that liposome after 6 cycles extruction and 10 minutes sonication showing the best evaluation for size distribution and entrapment efficiency. These liposome was also being proceed for gel formulation. Size distribution evaluation in gel showed that liposome size after 6 cycles of extruction has increased by 7,71 times and liposome size after 10 minutes sonication has increased by 12,18 times. Gel contained liposome after extruction had a better size reduction than gel contained liposome after sonication."

"ABSTRAKMinyak alga Botryococcus braunii merupakan sumber energi terbarukan. Kandungan minyak pada alga ini mencapai 75% biomassa keringnya. Kondisi pengekstrakan yang optimal dibutuhkan untuk mendapatkan minyak yang maksimal. Telah dilakukan penelitian tentang pengekstrakan minyak alga ini dengan metode sonikasi. Pelarut yang dicoba adalah air, n-hexane, methanol dan alkohol. Sedangkan, frekuensi sonikasi yang dipakai adalah + 40 kHz. Waktu sonikasi divariasikan pada saat proses ekstraksi, yaitu 15, 30 dan 45 menit. Hasilnya, pelarut yang bisa menghasilkan minyak adalah n-hexane, methanol dan alkohol. Minyak yang dihasilkan n-hexane sebesar 3%. Sedangkan dengan methanol, minyak yang didapatkan sebesar 21.25%. Untuk variasi waktu sonikasi 15, 30 dan 45 menit dengan pelarut methanol, minyak yang didapatkan adalah 21.25%, 13.75% dan 7.5%.

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ABSTRACTOil from the Botryococcus braunii algae is a renewable energy source. Oil content in this algae can reach 75% of its dry biomass. Optimal extraction conditions are required in order to obtain the maximum oil content. Research on algae oil extraction using sonication is done using distilled water, n-hexane, methanol and alcohol as solvents. Meanwhile, the sonication frequency used is + 40 kHz. Sonication time is varied during the extraction process, with 15-, 30-, and 45- minute intervals used. The results find that the solvents that can produce algae oil are n-hexane, methanol and alcohol. Oil yielded by the n-hexane solvent amounts to 3%. While with methanol, the amount of oil obtained is 21.25%. For sonication time variation with methanol solvent, the amount of oil obtained using 15-, 30-, and 45-minute intervals are 21.25%, 13.75% and 7.5% respectively"

"Propolis dikenal akan kandungan senyawa aktif berupa Flavonoid yang menunjukkan aktivitas antimikroba, antioksidan, antiinflamasi, dan antitumor. Namun, senyawa aktif tersebut memiliki stabilitas dan ketersediaan hayati terbatas yang mempengaruhi efek terapeutiknya. Maka, dilakukan enkapsulasi ekstrak propolis ke dalam liposom untuk mempertahankan karakteristik fungsionalnya. Enkapsulasi propolis ke dalam liposom dilakukan melalui thin film hydration, freeze thaw dan sonikasi. Sonikasi dilakukan untuk meratakan dan memperkecil ukuran liposom hingga diperoleh karakteristik yang ideal untuk meningkatkan kemampuan persebaran obat di dalam tubuh. Pada penelitian ini, diberikan variasi terhadap durasi sonikasi yang beragam dari 20, 30, hingga 40 menit untuk mengetahui pengaruhnya terhadap karakteristik liposom. Setiap variasi sampel tersebut akan melalui pengujian efisiensi enkapsulasi berbasis kandungan flavonoid, penentuan karakteristik liposom menggunakan Particle Size Analyzer (PSA), serta pengujian gugus fungsi menggunakan Fourier transform infrared (FTIR). Melalui uji ANOVA, diperoleh pengaruh yang signifikan antara durasi sonikasi terhadap efisiensi enkapsulasi dan karakteristik liposom. Jika dibandingkan, sampel C2 yang melalui sonikasi 30 menit memiliki karakteristik liposom yang terbaik, dimana ukuran partikel dan indeks polidispersitasnya masing-masing sebesar 115,667 ± 3,800 nm dan 0,309 ± 0,059. Sampel ini juga menunjukkan efisiensi enkapsulasi yang tinggi, yaitu mencapai 97,887 ± 0,025%.......Propolis is known for its active compounds in the form of Flavonoids which exhibit antimicrobial, antioxidant, anti-inflammatory, and antitumor activities. However, these active compounds have limited stability and bioavailability which affect their therapeutic effect. Thus, encapsulation of propolis extract into liposomes was carried out to maintain its functional characteristics. Propolis encapsulation into liposomes was carried out through thin film hydration, freeze thaw and sonication. Sonication was carried out to reduce and homogenize the size of the liposomes in order to improve drug delivery. In this study, various sonication durations were varied from 20, 30, and 40 minutes to determine the effect on liposome characteristics.  Each variation of the sample will be tested for encapsulation efficiency based on total flavonoids, determination of liposome characteristics using a Particle Size Analyzer (PSA), and functional group testing using Fourier transform infrared (FTIR). Through the ANOVA test, a significant effect was obtained between sonication duration on encapsulation efficiency and liposome characteristics. The C2 sample that was sonicated for 30 minutes had the best liposome characteristics, where the particle size and polydispersity index were 115.667 ± 3.800 nm and 0.309 ± 0.059, respectively. This sample also showed high encapsulation efficiency, which reached 97.887 ± 0.025%."