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"This research is to study the effects of _firing temperature and holding time on characteristics of Directed Metal Oxidation (DIMOAQ Ceramic Matrix Composites (CMCs) SiC /' A1 product. In this research, the firing temperature and holding time used are varied from 900° C to 1300° C with holding time 10 and 20 hours for each temperature. The characterizations of composite products are examined such as density and porosity test, micro hardness test, microstructure examination and chemical composition test. The results show that SiC preform has been infiltrated by Al liquid at tiring temperature of 1100"C for 20 hours. Composite product with the highest density (3,54 gram / cm3) can be obtained at firing temperature of 1100°C for 20 hours. Porosity tents to increase with increasing firing temperature. Composite product with highest micro hardness (1820 VHM can be obtained at firing temperature of 1300°C for 10 hours. At the some firing temperature, composite at products micro hardness for 20 hours tower than composite product with holding time I0 hours. Distribution of SiC particles spread over quite uniform on SiC/A1 composites product. Around SiC particles can be found Al, spinel (MgAl2O2). Al2O2, and possibility Mg,Si."

"Keramik merupakan material yang memiliki kekerasan yang sangat tinggi dan getas (getas). Untuk meningkatkan ketangguhan keramik,maka dikembangkan CMCs (Ceramic Matix Composite). Salah satu metode untuk memproduksi CMCs adalah dengan melalui proses DIMOX, yaitu cara mengoksida leburan logam dalam atmosfer dapur. Karakteristik produk CMCs yang dihasilkan melalui metode ini dipengaruhi oleh variabel waktu tahan, temperatur, dopant serta atmosfer tempat berlangsungnya proses pembentukan komposit.Penelitian ini bertujuan untuk mempelajari proses pembuatan CMCs C/Al melalui proses DIMOX dan pengaruh waktu tahan terhadap karakteristik produk CMCs yang dihasilkan. Pada penelitian ini dilakukan variasi waktu tahan, dimana digunakan waktu tahan 8, 10, 15, 20, 24 jam pada temperatur 1100 °C. Karakterisasi terhadap produk komposit yang dihasilkan dilakukan melalui pengujian densitas dan porositas, pengujian kekerasan mikro, pengamatan struktur mikro dengan menggunakan mikroskop optik dan SEM serta pegujian komposisi kimia.Infiltrasi prabentuk C oleh leburan Al dapat terjadi secara optimum pada waktu tahan 24 jam. Produk CMCs dengan densitas yang tertinggi, sebesar 3,17 gram/cm3, diperoleh pada waktu tahan 24 jam. Porositas produk CMCs cenderung meningkat seiring dengan penambahan waktu tahan. Produk CMCs dengan kekerasan mikro tertinggi, sebesar 14300 Mpa pada waktu tahan 24 jam. Laju keausan produk CMCs tertinggi, sebesar 2.03x10^-6 m3/mm terdapat pada waktu tahan 24 jam. Partikel C terdistribusi cukup merata pada produk CMC C/Al. Pada produk CMCs pada daerah sekitar partikel C dapat ditemui adanya Al, spinel (MgAl2O4), Al2O3.

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Ceramic is material which possed a very high hardness and brittle. To increase its toughness, then CMCs is developed. One of method to produce CMCs is DIMOX process. DIMOX involved oxidized molten metal in furnace atmosphere. The charateristic of CMCs product is effected by variables processes such as : holding time, temperature, dopant and the atmosphere where the process is held.

The aim of this research is to study the making process of CMCs C/Al itself through DIMOX process and the effect of holding time with variable : 8, 10, 15, 20, 24 hours at 1100 °C. The characterizations of CMCs are examined by density, porosity, hardness, wear and microstructure analysis.

It is found that Infiltration preform graphite by molten Al is optimal at the holding time of 24 hours. This variable produced highest density at 3,17 gr/cm3. The porosity of CMCs product tends to increase with increment of holding time. The highest porosity that obtained at holding time of 24 hours is 6.15 %. The highest hardness that can be obtained at holding time of 24 hours is 14300 MPa. This variable also produced the lowest wear rate, it is 2.03x10^-6 mm3/mm. Distribution of graphite particles spread over C / Al composite product and around graphite particles can be found Al, spinel ( MgAl2O4 ), and Al2O3. Based on EDS analysis, there are three phase in systems of CMCs product, they are C/Al, Al2O3/Al, and C/Al2O3."