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This research was intended to produce functionally graded material (FGM) of Hydroxyapatite (Hap)-silk fibroin by pulse electric current sintering in facing the need in biomaterial application. Silk sheet wasutilized as a bound between each layer. The target sample thickness was 1.6 mm with diameter I5 mm.Sample was created by using cylindrical type of carbon die and consisted of 4 layers with the samethickness in which silk film with the thickness of 100 ,tan was placed between the layers. The compositionof lower layer was l 00% silk fibroin, second layer was 90% silk fibroin + l 0% Hap, third layer was 80%silk fibroin + 20%Hap, and 70% silk fibroin + 30% Hap for the upper layer. The properties of FGM wascharacterized by optical microscope and scanning electron microscope (SEM). Three point bend withsingle-edge beam was used for _fracture toughness test (lim). The grade of the FGM material was provenby using electron probe micro analyzer (EPMA). The value of fracture toughness was 0. 65 l MPo.m".The silk film in the borders of the sample can arrest the crack perfectly, so that sudden fracture could beavoided The sample still remained capable supported the load after maximum load was reached Opticalmicrograph and SEM indicated that the Hap-silk fibroin FGM could be produced by using the methodthat was introduced in this research. |
