Synthesis of Nitro Derivative of 3-( 4--Chlorophenyl)-2-Methyl-Quinazolin-4- 0ne using Various Nitration Agents (article on The 2nd International Conference of the Indonesian Chemical Society October, 22-23 2013)
Steven Sastradi;
Maggadani, Baitha Palanggatan; Hayun
([Publisher not identified]
, 2013)
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ABSTRACT Nitration of 3-(4-cblorophenyl)-2-metbyl-quinazolin-4-oneusing various nitration agents have been performed. The purpose of the experiment wa,;toget the best nitl'lltion agentsforthe synthesis of nitro derivative ofthe compomtd. The various nitration agentsused were:fuming nitric acid-concentrated sulfuric acid, silver nitrate-N-bromosuccinimide (NBS). eerie ammoniwn nitrate-silica supported sulfuric acid, and eerie ammonium nincentrated sulfuric acid. The results showed that nitrationwithfumingnitricacickoncentrated sulfuricacid obtained 3-( 4'-chloro-3 '-nitropheny l}-2- methyl-6-nitro--quinazolin-4-onein49. 74%yield. Thestructurewas confirmedusing FT-IRand1H-NMR The other nitration methods were not give the desired results. |
MK-Hayun-Synthesis of Nitro.pdf :: Unduh
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No. Panggil : | MK-Pdf |
Entri utama-Nama orang : | |
Entri tambahan-Nama orang : | |
Entri tambahan-Nama badan : | |
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Penerbitan : | [Place of publication not identified]: [Publisher not identified], 2013 |
Bahasa : | eng |
Sumber Pengatalogan : | LibUI eng rda |
Tipe Konten : | text |
Tipe Media : | computer |
Tipe Carrier : | online resource |
Deskripsi Fisik : | 12 pages |
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Lembaga Pemilik : | Universitas Indonesia |
Lokasi : | Perpustakaan UI, Lantai 3 |
No. Panggil | No. Barkod | Ketersediaan |
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MK-Pdf | 10-18-135812948 | TERSEDIA |
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