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Intercalation of anthranilate ion into zinc-aluminium-layered double hydroxide

Eny Kusrini, Asmah Hj. Yahaya, Mohd Zobir Hussein , Zulkarnain Zainal (Faculty of Engineering, Universitas Indonesia, 2013)

 Abstrak

Nanocomposites of zinc-aluminium-anthranilate (ZAAN) have been synthesized at different concentrations of anthranilic acid by co-precipitation method. These materials have been examined in detail by powder X-ray powder diffraction (PXRD) which showed the expansion of the basal spacing from 0.89 to ca. 1.33 nm and the shifting of the 003 peak towards the lower 2q angle. This indicates that the anthranilate anion was successfully intercalated into the interlayer gallery. However, FTIR analysis showed nitrate anion was also co-intercalated in the interlayer. The resulting nanocomposites show Type IV adsorption-desorption isotherms indicated the mesoporous structure of the material. BET surface area was found to be slightly different compared to zinc-aluminium-nitrate-layered double hydroxide (ZANO) after the intercalation process took place. Both ZANO and ZAAN have similar surface morphology, namely a flaky-like structure, but they are of different sizes.

 Metadata

No. Panggil : UI-IJTECH 4:1 (2013)
Entri utama-Nama orang :
Subjek :
Penerbitan : Depok: Faculty of Engineering, Universitas Indonesia, 2013
Sumber Pengatalogan : LibUI eng rda
ISSN : 20869614
Majalah/Jurnal : International Journal of Technology
Volume : Vol. 4, No. 1, January 2013: Hal. 73-80
Tipe Konten : text
Tipe Media : unmediated
Tipe Carrier : volume
Akses Elektronik : https://doi.org/10.14716/ijtech.v4i1.99
Institusi Pemilik : Universitas Indonesia
Lokasi : Perpustakaan UI, Lantai 4 R. Koleksi Jurnal
  • Ketersediaan
  • Ulasan
No. Panggil No. Barkod Ketersediaan
UI-IJTECH 4:1 (2013) 08-23-79666890 TERSEDIA
Ulasan:
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